All issues Volume 71 / No 2 (March–April 2016) Oil Gas Sci. Technol. – Rev. IFP Energies nouvelles, 71 2 (2016) 20 Full HTMLActivity of the MoCl2(NO)2L2/AlEt3/PhOH for 4-nonyne metathesis
| Entry | 1 | 2 | 3 | 4 | 5 | 6 |
|---|---|---|---|---|---|---|
| L | Pyridine | NEt3 | PPh3 | P(OPh)3 | OPPh3 | None |
| TOF (h−1)a | 3300 | 4400 | 3950 | 3700c | 4750 | 3600d |
| TOF (h−1)b | 2150 | 3000 | 3650 | 2400c | 3800 | 3600d |
Conditions: T = 110°C; [C≡C]/[Mo] = 100; [AlEt3]/[Mo] = 6; PhOH/Mo = 100.
The use of a longer activation time was necessary (Tab. 2 below).
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